X-Ray Crystallography
The aim of this project is to use a narrow beam of X-Rays to produce an image/data that reflects the atomic and molecular structure of atoms in a crystal. The method used is called X-Ray crystallography where a narrow beam of X-rays is fired at a crystal, although most will pass straight through some of the x-rays are diffract by the lattice of atoms arranged in a crystal which sum and subtract to create an interference patterns at an angle to the main beam.
Crystals are regular arrays of atoms, and X-rays can be considered waves of electromagnetic radiation. Atoms scatter X-ray waves, primarily through the atoms' electrons. Just as an ocean wave striking a lighthouse produces secondary circular waves emanating from the lighthouse, so an X-ray striking an electron produces secondary spherical waves emanating from the electron. This phenomenon is known as elastic scattering, and the electron (or lighthouse) is known as the scatterer. A regular array of scatterers produces a regular array of spherical waves. Although these waves cancel one another out in most directions through destructive interference, they add constructively in a few specific directions, determined by Bragg 's law: 2d \sin \theta = n \lambda
I bought an X-ray tube for this project, to provide a narrow beam of x-rays. It's called a diffraction transmitting target x-ray tube made in Soviet Russian times during the 1990s type BS7-W. As it turned out the design of this tube is quite unusual, but nevertheless it works quite well and produces a fine beam of soft x-rays and a little more safer than other tubes to work with.
More details about this here: X-ray tube - diffraction transmitting target (Russian BS7-W)
As the tube requires a modest operating voltage of 15Kv and current for the Anode and a small voltage of 1.5V for the filament the power supply t was relatively easy to construct using commonly available components.
Here is the first test of the tube in operation. The Geiger Counter is first checked against other radioactive sources to gauge roughly relative output levels.
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X-ray tube - diffraction transmitting target (Russian BS7-W)
I bought the above X-ray tube for a X-Ray crystallography project I'm currently working on - It's called a diffraction transmitting target x-ray tube made in Soviet Russian times during the 1990s type BS7-W. They are available from a store in the Ukraine called Soviet Radio Components.
Unfortunatly the english translated datasheet isn't that helpful other than some operating numbers.
- Operating voltage is 10kV max 15kV
- Filament voltage is 1.2V max 1.5V
- Beam is 5 degrees
As there is no pin out information either, my first attempts to use the tube had mixed results. Nevertheless I was able to able to produce quite a nice fine beam of x-rays before blowing the filament.
Although blowing the filament wasn’t really the best result, it did give me the opportunity to break open the tube and find out how it ticked. As it turned out this was a very worthwhile and interesting process, because it was not built in a way I expect almost the reverse. I was also left with a Beryllium x-ray window which I can use for the light screen in an x-ray detector.
The design of this x-ray tube is quite the reverse of most x-ray tubes I've seen, nevertheless it does produce a fine beam of
x-rays. But how it does this is a bit mysterious.
Typical x-ray tube
In a typical x-ray tube, X-rays are produced when a beam of electrons emitted by a filament in the Cathode are accelerated by a high voltage potential between the Cathode and Anode. The beam of electrons produced hit the Anode and are suddenly decelerated upon collision with the atoms in the metal Anode.
These x-rays are commonly called brehmsstrahlung or "braking radiation". If the bombarding electrons have sufficient energy, they can knock an electron out of an inner shell of the Anodes metal atoms. Then electrons from higher states drop down to fill the vacancy, emitting x-ray photons with precise energies determined by the electron energy levels.
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